ГОСТ Р ИСО 16634-1-2011 Продукты пищевые. Определение общего содержания азота путем сжигания по методу Дюма и расчет содержания сырого протеина. Часть 1. Масличные культуры и корма для животных (Переиздание)

[1]

ISO 542

Oilseeds - Sampling

[2]

ISO 1871

Food products - General guidelines for the determination of nitrogen by the Kjeldahl method

[3]

ISO 5500

Oilseed residues - Sampling

[4]

ISO 5725-1

Accuracy (trueness and precision) of measurement methods and results - Part 1: General principles and definitions

[5]

ISO 5725-2

Accuracy (trueness and precision) of measurement methods and results - Part 2: Basic method for the determination of repeatability and reproducibility of a standard measurement method

[6]

ISO 5983-1

Animal feeding stuffs - Determination of nitrogen content and calculation of crude protein content - Part 1: Kjeldahl method

[7]

ISO 5983-2

Animal feeding stuffs - Determination of nitrogen content and calculation of crude protein content - Part 2: Block digestion/steam distillation method

[8]

ISO 6497

Animal feeding stuffs - Sampling

[9]

ISO 13690

Cereals, pulses and milled products - Sampling of static batches

[10]

ISO 148911/IDF 185

Milk and milk products - Determination of nitrogen content - Routine method using combustion according to the Dumas principle

[11]

ISO 20483

Cereals and pulses - Determination of the nitrogen content and calculation of the crude protein content - Kjeldahl method

[12]

ICC Standard No. 167, Determination of crude protein in grain and grain products for food and feed by the Dumas combustion principle

[13]

AACC approved method 46-30: Crude protein - Combustion method. In: AACC approved methods. American Association of Cereal Chemists, St. Paul, MN, 2002. Available (2008-04-08) from http://www.aaccnet.org

[14]

 AOAC official method 992.23: Crude protein in cereal grains and oilseeds. In: Official methods of analysis of AOAC International. AOAC International, Washington, DC, 2002. Available (2008-04-08) from http://eoma.aoac.org

[15]

 AOAC official method 997.09: Nitrogen in beer, wort, and brewing grains: Protein (total) by calculation - Combustion method. ASBC-AOAC Method. In: Official methods of analysis of AOAC International. AOAC International, Washington, DC, 2002. Available (2008-04-08) from http://eoma.aoac.org

[16]

AOAC official method 990.03: Protein (crude) in animal feed. Combustion method. In: Official methods of analysis of AOAC International. AOAC International, Washington, DC, 2002. Available (2008-04-08) from http://eoma.aoac.org

[17]

AOCS official method Ba 4f-00: Combustion method for determination of crude protein in soybean meal. In: Official methods and recommended practices of the AOCS, FIRESTONE, D.E., editor. AOCS Press, Champaign, IL, 1997. Available (2008-04-08) from http://www.aocs.org

[18]

AOCS official method Ba 4e-93: Generic combustion method for determination of crude protein. In: Official methods and recommended practices of the AOCS, FIRESTONE, D.E., editor. AOCS Press, Champaign, IL, 1997. Available (2008-04-08) from http://www.aocs.org

[19]

AOCS official method Bc 4-91: Nitrogen-ammonia-protein modified Kjeldahl method titanium oxide + copper sulfate catalyst. In: Official methods and recommended practices of the AOCS, FIRESTONE, D.E., editor. AOCS Press, Champaign, IL, 1997. Available (2008-04-08) from http://www.aocs.org

[20]

BERNER D.L., BROWN J. Protein nitrogen combustion method collaborative study: 1 - Comparison with Smalley total Kjeldahl nitrogen and combustion results. J. Am. Oil Chem. Soc. 1994, 71, p.1291-1293

[21]

BICSAK R.C. Comparison of Kjeldahl method for determination of crude protein in cereal grains and oilseeds with generic combustion method: Collaborative study. J. AOAC Int. 1993, 76, p.780-786

[22]

BUCKEE G.K. Determination of total nitrogen in barley, malt and beer by Kjeldahl procedures and the Dumas combustion method - Collaborative trial. J. Inst. Brew. 1994, 100, p.57-64

[23]

DAUN J.K., DECLERCQ D.R. Comparison of combustion and Kjeldahl methods for determination of nitrogen in oilseeds. J. Am. Oil Chem. Soc. 1994, 71, p.1047-1078

[24]

DONHAUSER S., GEIGER E., BRIEM F. Automatic nitrogen measurement using a combustion method. Brauwelt Int. 1993, (3), p.219-221

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ELLEN G., MAHULETTE G.G. Stikstofbepaling in zuivelproducten: Dumas evenaart Kjeldahl [Nitrogen determination in dairy products: Dumas equals Kjeldahl]. Voedingsmiddelen-technol. 1997, 30 (3), p.25-29

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ETHERIDGE R.D., PESTI G.M., FOSTER E.H.A. A comparison of nitrogen values obtained utilizing the Kjeldahl nitrogen and Dumas combustion methodologies (Leco CNS 2000) on samples typical of an animal nutrition analytical laboratory. Animal Feed Sci. Technol. 1998, 73, p.21-28

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FOSTER A. Alternative method for analysis of total protein using the nitrogen determinator. J. Am. Soc. Brew. Chem. 1989, 47, p.42-43

[28]

FRISTER H., FEIER U., GOETSCH P.-H. Direct determination of nitrogen content by Dumas analysis: Interlaboratory study on precision characteristics. AOAC International - Europe Section, 4th International Symposium, Nyon, Switzerland, 1994

[29]

JOHANSSON C.-G. Determination of total nitrogen in barley and malt by combustion method: Collaborative trial. Monatsschr. Brauwiss. 1996, 49, p.326-330

[30]

KINGBRINK M., SEBRANEK J.G. Combustion method for determination of crude protein in meat and meat products: Collaborative study. J. AOAC Int. 1993, 76, p.787-793

[31]

REVESZ R.N., AKER N. Automated determination of protein-nitrogen in cereals and grains. J.Assoc. Off. Anal. Chem. 1977, 60, p.1238-1242

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SCHUSTER M., MORWARID M., SATTES, H. [The determination of the protein content in feedstuffs by the Dumas method]. In: 103. VDLUFA-Kongress, Ulm, Germany, 1991-09-16 to 21, p.526-531. VDLUFA, Darmstadt

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SMITH I.D. Evaluation of the Foss-Heraeus macro N for the determination of nitrogen in a wide range of foodstuffs, ingredients and biological materials and comparison with the Kjelfoss. Anal. Proc. 1991, 28, p.320-324

[34]

SWEENEY R.A. Generic combustion method for determination of crude protein in feeds: Collaborative study. J. Assoc. Off. Anal. Chem. 1989, 72, p.770-774

[35]

TKACHUK R. Nitrogen-to-protein conversion factors for cereals and oilseed meals. Cereal Chem. 1969, 46, p.419-423

[36]

WINKLER R., BOTTERBRODT S., RABE E., LINDHAUER M.G. Stickstoff-/Proteinbestimmung mit der Dumas-Methode in Getreide und Getreideprodukten [Nitrogen/protein determination in wheat and wheat products (flour and meal) by the Dumas method]. Getreide Mehl Brot 2000, 54, p.86-91

[37]

JOINT FAO/WHO AD HOC EXPERT COMMITTEE ON ENERGY AND PROTEIN REQUIREMENTS. Energy and protein requirements: Report of a Joint FAO/WHO Ad Hoc Expert Committee, Rome, 22 March-2 April 1971. Rome, Food and Agriculture Organization, 1973. 118 p. (FAO Nutrition Meetings Report, No. 52; WHO Technical Report, No. 522.)

[38]

BELLOMONTE G., COSTANTINI A., GIAMMARIOLI S. Comparison of modified automatic Dumas method and the traditional Kjeldahl method for nitrogen determination in infant food. J. Assoc. Off. Anal. Chem. 1987, 70, p.227-229

[39]

JUNG S., RICKERT D.A., DEAK N.A., ALDIN E.D., RECKNOR J., JOHNSON L.A., MURPHY P.A. Comparison of Kjeldahl and Dumas methods for determining protein contents of soybean products. J. Am. Oil Chem. Soc. 2003, 80, p.1169-1173

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SCHMITTER B.M., RIHS T. Evaluation of a macrocombustion method for total nitrogen determination in feedstuffs. J. Agric. Food Chem. 1989, 37, p.992-994

[41]

SIMONNE A.H., SIMONNE E.H., EITENMILLER R.R., MILLS H.A., CRESMAN C.P Could the Dumas method replace the Kjeldahl digestion for nitrogen and crude protein determinations in foods? J. Sci. Food Agric. 1997, 73, p.39-45

[42]

SWEENEY R.A., REXROAD P.R. Comparison of LECO FP-228 "nitrogen determinator" with AOAC copper catalyst Kjeldahl method for crude protein. J. Assoc. Off. Anal. Chem. 1987, 70, p.1028-1030

[43]

WILES P.G., GRAY I.K., KISSLING R.C. Routine analysis of proteins by Kjeldahl and Dumas methods: Review and interlaboratory study using dairy products. J. AOAC Int. 1998, 81, p.620-632

УДК 663/664.777:006.354

ОКС 65.120

67.050

67.200

Ключевые слова: масличные культуры, корма для животных, общее содержание азота, метод Дюма, расчет содержания сырого протеина, термины и определения, подготовка к определению, расчет и обработка результатов, прецизионность